Acid Baking Rare Earth Elements

Resistant rare earth phosphates as possible sources of …

Global demand for rare earth elements (REE; lanthanides plus Y and Sc), particularly heavy rare earth elements (HREE; from Gd to Lu), has rocketed due to their wide applications in advanced technologies (e.g., permanent magnets, super metal alloys, catalysts, etc.) (Hatch, 2012).REE are increasingly considered critical and strategic metals owing to their …


Sulfuric Acid Baking and Leaching of Rare Earth Elements, …

Monazite, a rare earth and thorium phosphate mineral, is one of the major minerals processed for extraction of rare earths. Industry practice for treating monazite concentrates is to use either a sulfuric acid bake or caustic conversion route. In the sulfuric acid bake, monazite concentrate is mixed with concentrated sulfuric acid and roasted. The rare earth phosphate mineral is …


The impact of apatite on sulfuric acid baking of a monazite …

Sulfuric acid baking of monazite ((Ce,La,Th)PO 4) bearing ores is one of the major processes used in commercial production of rare earth elements.In hydrothermal vein type rare earth deposits, apatite is often found together with monazite.Rare earth enriched fluorapatite ores may also contain significant amounts of rare earths hosted in monazite. An understanding of …


An acid baking approach to enhance heavy rare earth …

In this study, the mechanism of calcination-acid leaching for rare earth elements (REY) recovery from coal gangue of Jungar coalfield was proposed based on the results of …


An acid baking approach to enhance heavy rare earth …

The recovery of rare earth elements (REEs) from secondary resources, particularly coal-based materials, has recently received attention due to supply and demand imbalance. ... Sulfuric acid baking and leaching of rare earth elements, thorium and phosphate from a monazite concentrate: Effect of bake temperature from 200 to 800 °C. Demol, John ...


Leaching and recovery of phosphate and rare earth elements …

Semantic Scholar extracted view of "Leaching and recovery of phosphate and rare earth elements from an iron-rich fluorapatite concentrate: Part II: Selective leaching of calcium and phosphate and acid baking of the residue" by Faraz Soltani et al.


Selective Nitric Acid Leaching of Rare-Earth Elements from …

Esfordi phosphate concentrate (Yazd Province, Iran) contains 13.1% P, 34.6% Ca, and 1.09% rare-earth elements (REEs), being one of the most important sources of REEs in Iran. REEs can be extracted from phosphate concentrates as a by-product of phosphoric acid production processes. In this work, nitric acid was used for leaching of REEs and phosphate …


Sulfuric Acid Baking and Leaching of Rare Earth Elements

Results from SEM -EDS analysis of the sample after acid baking at 300 °C showed that the rare earth elements were present as sulfates, while thorium was present in an amorphous phosphate type phase. In the leach residue, thorium was also present as a phosphate type species, but with a significantly different composition and appearance to the ...


Sulfuric Acid Leaching Recovery of Rare Earth Elements from …

Rare earth elements (REEs) are considered vital raw materials for the economy and are on the European Union's list of critical raw materials (CRMs). Europe is mainly dependent …


ect of Sulfuric Acid Baking and Caustic Digestion on …

minerals Article E ect of Sulfuric Acid Baking and Caustic Digestion on Enhancing the Recovery of Rare Earth Elements from a Refractory Ore Rina Kim 1,*, Heechan Cho 2, Jinan Jeong 2, Jihye Kim 3, Sugyeong Lee 4, Kyeong Woo Chung 1, Ho-Sung Yoon 1 and Chul-Joo Kim 1 1 Resources Recovery Research Center, Mineral Resources Division, Korea Institute of …


Application of deep eutectic solvents (DESs) as a green …

For centuries, humanity has acquired the necessary natural resources of metals through ore mining and mineral processing. In the modern era, as a result of technological advancement and population growth, the need for primary manufacturing resources has surged [1], [2].Rare earth elements (REEs), or in concise rare earth, are a category of 15 …


Sulfuric acid baking and water leaching of rare earth elements …

Semantic Scholar extracted view of "Sulfuric acid baking and water leaching of rare earth elements from coal tailings" by V. Kuppusamy et al. ... Parametric study of an acid baking process for rare earth element recovery from a bituminous …


Parametric study of an acid baking process for rare earth element

DOI: 10.1080/19392699.2023.2269094 Corpus ID: 264103337; Parametric study of an acid baking process for rare earth element recovery from a bituminous-coal source @article{Nawab2023ParametricSO, title={Parametric study of an acid baking process for rare earth element recovery from a bituminous-coal source}, author={Ahmad Nawab and Xinbo …


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Although sulfuric acid baking is one of the main processing routes for extraction of rare earth elements from monazite, the chemistry involved is not well understood. In this study, a combination of chemical analysis and standard characterisation techniques (XRD, SEM-EDS, FT-IR and TG-DSC) was used to identify reaction processes occurring ...


Evaluating organic acids as alternative leaching reagents for rare …

This study proposes an advanced leaching method using organic acids to recover rare earth elements (REEs) from NdFeB permanent magnets from end-of-life computers hard disk drives (HDDs). The end-of-life HDDs were first dismantled in order to recover NdFeB magnets, which were then thermally demagnetized at 350 °C during 30 min before crushing in …


The sulfuric acid bake and leach route for processing of rare earth

The work investigates the effect of sulfuric acid baking on rare earth element (REE) extraction from two waste rock samples from a phosphate mine. The role of different mineralogical assemblages and … Expand. 2. PDF. Save. Extraction of Rare-Earth Elements from Silicate-Based Ore through Hydrometallurgical Route.


Parametric study of an acid baking process for rare earth element

Monazite, a rare earth and thorium bearing phosphate mineral, is one of the major minerals used for the production of rare earth elements. Although sulfuric acid baking is one of the main ...


Sulfuric acid baking and water leaching of rare earth elements …

Sulfuric acid baking followed by water leaching (ABWL) is a conventional way to extract rare earth elements (REEs) from traditional REE ore deposits.


The Effect of Iron- and Calcium-Rich Waste Rock's Acid Baking …

The work investigates the effect of sulfuric acid baking on rare earth element (REE) extraction from two waste rock samples from a phosphate mine. The role of different mineralogical assemblages and the degree of alteration (i.e., weathering), and the behavior of the main impurities–iron, phosphorus, and calcium–on REE extraction are emphasized.


Recovery of lanthanum and cerium from rare earth …

Baking with the concentration sulfuric acid at 300 °C, the rare earth elements were converted into the La(III) sulfate and Ce(IV) sulfate phase, which indicates the complete transformation of lanthanum/cerium oxide to the La/Ce-sulfate salt …


Sulfuric Acid Leaching of Heavy Rare Earth Elements …

A sieving process was carried out since it was known that most heavy rare earth elements (HREEs) content occurs at a larger size. The alkaline fusion process was applied with an intent to break the phosphate bonds present in the REE-carrying minerals (xenotime and monazite) and convert phosphate bonds to hydroxide bonds in rare earth metals.


LEACHING OF RARE EARTH ELEMENTS: PAST AND …

Bastnaesite is a rare earth fluorocarbonate mineral1, RE(CO3)F, which primarily contains light rare earth elements. After physical upgrading, bastnaesite ore concentrates contain between 40 to 60% REE2. One of the main concerns in past bastnaesite processing technologies (see …


A Critical Review of the Enhanced Recovery of Rare Earth …

The increasing demand for rare earth elements (REEs), especially from new and innovative technology, has strained their supply, which makes the exploration of new REE …


The Effect of Iron- and Calcium-Rich Waste Rock's …

The work investigates the effect of sulfuric acid baking on rare earth element (REE) extraction from two waste rock samples from a phosphate mine. The role of different mineralogical assemblages and the degree of …


Parametric study of an acid baking process for rare earth element

Parametric study of an acid baking process for rare earth element recovery from a bituminous-coal source Buy Article: $71.00 + tax (Refund Policy) Authors: Nawab 1; Yang 2; Honaker 1; Source: International Journal of Coal Preparation and Utilization, Volume ...


Sulfuric Acid Leaching Recovery of Rare Earth Elements …

Rare earth elements (REEs) are considered vital raw materials for the economy and are on the European Union's list of critical raw materials (CRMs). Europe is mainly dependent on REE imports. This dependence could be reduced if locally available primary or secondary resources would be processed. In Poland, there are, for instance, over 5 million metric tons of …


Effect of Sulfuric Acid Baking and Caustic Digestion on …

To improve the recovery of rare earth elements (REEs) from a refractory ore, this study investigated two different chemical decomposition methods, namely sulfuric acid baking and caustic digestion, with their respective leaching processes. The studied lateritic ore contained goethite (FeOOH) as a major constituent with REEs scattered around and forming submicron …


CHARACTERIZATION AND EXTRACTION OF RARE …

Sulfuric acid baking and water leaching of rare earth elements from coal tailings. Fuel, 319(123738). DOI: 10.1016/j.fuel.2022.123738. o I was responsible for the conceptualization, methodology, investigation, and writing—original draft, review, and editing. ... rare earth elements in the east Kootenay coalfields of southeastern British ...


‪Gisele Azimi‬

Process investigation of the acid leaching of rare earth elements from phosphogypsum using HCl, HNO3, and H2SO4. M Walawalkar, CK Nichol, G Azimi. Hydrometallurgy 166, 195-204, 2016. 189: ... Recovery of scandium from Canadian bauxite residue utilizing acid baking followed by water leaching. J Anawati, G Azimi. Waste management 95, 549-559 ...


Sulfuric Acid Baking and Leaching of Rare Earth …

In the sulfuric acid bake, monazite concentrate is mixed with concentrated sulfuric acid and roasted. The rare earth phosphate mineral is converted to rare earth sulfate which dissolves in …